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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1065176Generated: October 27, 2026

Sulfuric Acid → 3-(4-Cyclohexylphenyl)-2-methylpropyl chloride

https://huagongshe.com/reaction/1065176

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSulfuric AcidHCID 1118—
ReactantCyclohexeneHCID 8079—
Reactant(3-Chloro-2-methylpropyl)benzeneHCID 13510156—
SolventChloroformHCID 6212—
Product3-(4-Cyclohexylphenyl)-2-methylpropyl chlorideHCID 2054157570%

Reaction Steps

33 parts by weight of cyclohexene are added dropwise to a mixture of 67 parts by weight of 2-methyl-3-phenylpropyl chloride and 40 parts by weight of 96% strength sulfuric acid at 10° C. Stirring is continued for 14 hours at room temperature. The crude product is dissolved in CHCl3 and the solution is thoroughly washed with ice water, dried over Na2CO3 and distilled. 70 parts by weight of 3-(4-cyclohexylphenyl)-2-methyl-propyl chloride are obtained; boiling point 130° C.-2° C./0.1 mm Hg, yield 70% (based on 2-methyl-3-phenylpropyl chloride).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04328380
Source datasetuspto-grants-1982_05
ORD IDord-3ac2beb5a31147eb819c6081e2818b11
Source noteuspto-grants-1982_05