HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4,5,6-Tetrahydrophthalic anhydride → HCID 20541555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4,5,6-Tetrahydrophthalic anhydride | HCID 12475 | — |
| Reactant | 4-Chloro-2-fluoroaniline | HCID 93898 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20541555 | HCID 20541555 | — |
Reaction Steps
3,4,5,6-tetrahydrophthalic anhydride (7.7 g) and 2-fluoro-4-chloroaniline (7.2 g) were added to acetone (50 ml) and, after stirring at 50°-55° C. for 5 minutes, the reaction mixture was concentrated under reduced pressure. The resultant crystals were washed with n-hexane. Yield 13.2 g; m.p. 92°-94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04328367 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-02da71f5a42d463fbc239880564cdc9f |
| Source note | uspto-grants-1982_05 |