3,4-Dimethoxybenzene-1-thiol → HCID 20260655, compound

HRID 1065327Notes

Reaction equation

HRID 1065327 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([SH:11])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10].Cl[CH2:13][CH2:14][CH2:15][CH2:16][O:17][C:18]1[CH:19]=[C:20]2[C:25](=[CH:26][CH:27]=1)[NH:24][C:23](=[O:28])[CH2:22][CH2:21]2.OC1C=C2C(=CC=1)NC(=O)C=C2.C1(S(OCCCCCl)(=O)=O)C=CC=CC=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([S:11][CH2:13][CH2:14][CH2:15][CH2:16][O:17][C:18]2[CH:19]=[C:20]3[C:25](=[CH:26][CH:27]=2)[NH:24][C:23](=[O:28])[CH2:22][CH2:21]3)[CH:6]=[CH:7][C:8]=1[O:9][CH3:10]

Participants

5

Reactant 4

HCID 1365393,4-Dimethoxybenzene-1-thiolHCID 1770652,6-DihydroxyquinolineHCID 20540073HCID 20540073, compoundHCID 88753054HCID 88753054, compound

Product 1

HCID 20260655HCID 20260655, compound

Procedure

Prepared analogous to Example 1 from 3,4-dimethoxy-thiophenol and 6-(4-chlorobutoxy)-3,4-dihydro-carbostyril [prepared from 6-hydroxy-carbostyril (see F. Mayer et al. in Ber. Dtsch. Chem. Ges. 60, 858 (1927) and 4-chloro-butyl benzenesulfonate].

Sources & evidence

ORD record
ord-be8f5d1f0016477fa0bee75b702e2730
Source dataset
uspto-grants-1982_05
Patent number
US04329347

Reaction notes

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