2,6-Di-tert-butyl-4-mercaptophenol → 6-[4-(4-Hydroxy-3,5-di-tert. butylphenyl-mercapto)-butoxy]-carbostyril

HRID 1065415Notes

Reaction equation

HRID 1065415 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[C:9]2[C:14](=[CH:15][CH:16]=1)[NH:13][C:12](=[O:17])[CH:11]=[CH:10]2.[OH:18][C:19]1[C:24]([C:25]([CH3:28])([CH3:27])[CH3:26])=[CH:23][C:22]([SH:29])=[CH:21][C:20]=1[C:30]([CH3:33])([CH3:32])[CH3:31]>>[OH:18][C:19]1[C:20]([C:30]([CH3:31])([CH3:32])[CH3:33])=[CH:21][C:22]([S:29][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]2[CH:8]=[C:9]3[C:14](=[CH:15][CH:16]=2)[NH:13][C:12](=[O:17])[CH:11]=[CH:10]3)=[CH:23][C:24]=1[C:25]([CH3:28])([CH3:27])[CH3:26]

Participants

3

Reactant 2

HCID 703702,6-Di-tert-butyl-4-mercaptophenolHCID 152906936-(4-Bromobutoxy)quinolin-2(1H)-one

Product 1

HCID 887561266-[4-(4-Hydroxy-3,5-di-tert. butylphenyl-mercapto)-butoxy]-carbostyril

Procedure

Prepared analogous to Example 122 from 6-(4-bromobutoxy)-carbostyril (m.p. 198°-199° C.) and 4-hydroxy-3,5-di-tert. butyl-thiophenol (m.p. 84.5°-86.0° C.).

Sources & evidence

ORD record
ord-83d04e8f56844a47a50c280b4435765c
Source dataset
uspto-grants-1982_05
Patent number
US04329347

Reaction notes

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