2,4,5-Trichlorobenzenethiol → 6-[4-(2,4,5-Trichlorophenyl-mercapto)-butoxy]-carbostyril

HRID 1065430Notes

Reaction equation

HRID 1065430 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[C:9]2[C:14](=[CH:15][CH:16]=1)[NH:13][C:12](=[O:17])[CH:11]=[CH:10]2.[Cl:18][C:19]1[CH:24]=[C:23]([Cl:25])[C:22]([Cl:26])=[CH:21][C:20]=1[SH:27]>>[Cl:18][C:19]1[CH:24]=[C:23]([Cl:25])[C:22]([Cl:26])=[CH:21][C:20]=1[S:27][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[C:9]2[C:14](=[CH:15][CH:16]=1)[NH:13][C:12](=[O:17])[CH:11]=[CH:10]2

Participants

3

Reactant 2

HCID 195972,4,5-TrichlorobenzenethiolHCID 152906936-(4-Bromobutoxy)quinolin-2(1H)-one

Product 1

HCID 205399766-[4-(2,4,5-Trichlorophenyl-mercapto)-butoxy]-carbostyril

Procedure

Prepared analogous to Example 122 from 6-(4-bromobutoxy)-carbostyril (m.p. 198°-199° C.) and 2,4,5-trichlorothiophenol.

Sources & evidence

ORD record
ord-878dc56ec5bc4432aba5b0335f53e61b
Source dataset
uspto-grants-1982_05
Patent number
US04329347

Reaction notes

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