3,4-Dichlorobenzenethiol → 6-[3-(3,4-Dichlorophenyl-mercapto)-propoxy]-3,4-dihydro-carbostyril

HRID 1065442Notes

Reaction equation

HRID 1065442 reaction equation
Br[CH2:2][CH2:3][CH2:4][O:5][C:6]1[CH:7]=[C:8]2[C:13](=[CH:14][CH:15]=1)[NH:12][C:11](=[O:16])[CH2:10][CH2:9]2.[Cl:17][C:18]1[CH:19]=[C:20]([SH:25])[CH:21]=[CH:22][C:23]=1[Cl:24]>>[Cl:17][C:18]1[CH:19]=[C:20]([S:25][CH2:2][CH2:3][CH2:4][O:5][C:6]2[CH:7]=[C:8]3[C:13](=[CH:14][CH:15]=2)[NH:12][C:11](=[O:16])[CH2:10][CH2:9]3)[CH:21]=[CH:22][C:23]=1[Cl:24]

Participants

3

Reactant 2

HCID 799643,4-DichlorobenzenethiolHCID 13055728HCID 13055728, compound

Product 1

HCID 205400026-[3-(3,4-Dichlorophenyl-mercapto)-propoxy]-3,4-dihydro-carbostyril

Procedure

Prepared analogous to Example 122 from 6-(3-bromopropoxy)-3,4-dihydro-carbostyril (m.p. 111°-118° C.) and 3,4-dichloro-thiophenol.

Sources & evidence

ORD record
ord-32724a4e74d74b14acea817faf80267e
Source dataset
uspto-grants-1982_05
Patent number
US04329347

Reaction notes

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