3,4-Dichlorobenzenethiol → HCID 20540033, compound

HRID 1065452Notes

Reaction equation

HRID 1065452 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][O:7][C:8]1[CH:9]=[C:10]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[CH2:12][CH2:11]2.[Cl:19][C:20]1[CH:21]=[C:22]([SH:27])[CH:23]=[CH:24][C:25]=1[Cl:26]>>[Cl:19][C:20]1[CH:21]=[C:22]([S:27][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][O:7][C:8]2[CH:9]=[C:10]3[C:15](=[CH:16][CH:17]=2)[NH:14][C:13](=[O:18])[CH2:12][CH2:11]3)[CH:23]=[CH:24][C:25]=1[Cl:26]

Participants

3

Reactant 2

HCID 799643,4-DichlorobenzenethiolHCID 20540059HCID 20540059, compound

Product 1

HCID 20540033HCID 20540033, compound

Procedure

Prepared analogous to Example 122 from 6-(5-bromopentoxy)-3,4-dihydro-carbostyril (m.p.: 97°-98° C.) and 3,4-dichloro-thiophenol.

Sources & evidence

ORD record
ord-b27513c6fa474580b0dba58930d23de3
Source dataset
uspto-grants-1982_05
Patent number
US04329347

Reaction notes

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