Thiophenol → HCID 53652081, compound

HRID 1065457Notes

Reaction equation

[N+:1]([C:4]1[C:13]([O:14][CH2:15][CH2:16][CH2:17][CH2:18]Br)=[CH:12][CH:11]=[C:10]2[C:5]=1[CH:6]=[CH:7][C:8](=[O:20])[NH:9]2)([O-:3])=[O:2].[C:21]1([SH:27])[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[N+:1]([C:4]1[C:13]([O:14][CH2:15][CH2:16][CH2:17][CH2:18][S:27][C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)=[CH:12][CH:11]=[C:10]2[C:5]=1[CH:6]=[CH:7][C:8](=[O:20])[NH:9]2)([O-:3])=[O:2]

Participants

Reactant 2

HCID 7969Thiophenol

HCID 20540100HCID 20540100, compound

Product 1

HCID 53652081HCID 53652081, compound

Procedure

Prepared analogous to Example 122 from 5-nitro-6-(4-bromo-butoxy)-carbostyril [m.p. 250° C., prepared by nitration of 6-(4-bromo-butoxy)-3,4-dihydro-carbostyril] and thiophenol.

Sources & evidence

ORD record: ord-163a80ab8d724703b96119af53e62f17
Source dataset: uspto-grants-1982_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04329347

Reaction notes

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