反应详情

The 3-(acetylthio)-2-(methylthio)propionic acid is refluxed in thionyl chloride for two hours. The reaction mixture is distilled to remove excess thionyl chloride and the product is distilled in vacuo to yield 3-(acetylthio)-2-(methylthio)propionic acid chloride.

1. distillationThe reaction mixture is distilled
2. customto remove excess thionyl chloride
3. distillationthe product is distilled in vacuo