Thionyl Chloride → HCID 12800625, compound

Participants

Reaction Steps

The compound (3) (1.1 g) was dissolved in 20 ml of benzene, and 2 ml of thionyl chloride was added dropwise at room temperature with stirring. Then, the mixture was refluxed with stirring. The reaction mixture was concentrated, and n-hexane was added to the concentrate to crystallize it. The resulting crystals wer collected by filtration, washed with n-hexane and dried to afford 980 mg of the desired product.

Provenance & Evidence