Benzene, 2-chloro-1,5-dinitro-3-(trifluoromethyl)- → HCID 13043901, compound

HRID 1065778Notes

Reaction equation

HRID 1065778 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH3:9])=[CH:4][N:3]=1.[N+:10]([C:13]1[CH:18]=[C:17]([N+:19]([O-:21])=[O:20])[CH:16]=[C:15]([C:22]([F:25])([F:24])[F:23])[C:14]=1Cl)([O-:12])=[O:11]>>[CH3:9][O:8][C:5]1[CH:6]=[CH:7][C:2]([NH:1][C:14]2[C:15]([C:22]([F:24])([F:25])[F:23])=[CH:16][C:17]([N+:19]([O-:21])=[O:20])=[CH:18][C:13]=2[N+:10]([O-:12])=[O:11])=[N:3][CH:4]=1

Participants

3

Reactant 2

HCID 67851Benzene, 2-chloro-1,5-dinitro-3-(trifluoromethyl)-HCID 113209342-Amino-5-methoxypyridine

Product 1

HCID 13043901HCID 13043901, compound

Procedure

In accordance with the process of Preparation 8 except using 1.2 g. of 2-amino-5-methoxypyridine and 2.8 g. of 2,4-dinitro-6-trifluoromethylchlorobenzene, the reaction was carried out for 5 hours. The reaction mixture was treated as the process of Preparation 6 to obtain 1.2 g. of the object compound having the melting point of 102° to 105° C.

Workup

  1. customIn accordance with the process of Preparation 8
  2. additionThe reaction mixture was treated as the process of Preparation 6
  3. customto obtain 1.2 g

Sources & evidence

ORD record
ord-f26b5141af1c40e1a9459d816071eab7
Source dataset
uspto-grants-1982_05
Patent number
US04331670

Reaction notes

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