HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-5-(trifluoromethyl)-2-pyridinamine → N-(3-chloro-5-trifluoromethyl-2-pyridyl)-2,4-dinitro-3-methoxy-6-trifluoromethylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-5-(trifluoromethyl)-2-pyridinamine | HCID 607248 | — |
| Reactant | 2,4-Dinitro-3-methoxy-6-trifluoromethylchlorobenzene | HCID 20538589 | — |
| Product | N-(3-chloro-5-trifluoromethyl-2-pyridyl)-2,4-dinitro-3-methoxy-6-trifluoromethylaniline | HCID 13043913 | — |
Reaction Steps
In accordance with the process of Preparation 8 except using 1.9 g. of 2-amino-3-chloro-5-trifluoromethylpyridine and 2.8 g. of 2,4-dinitro-3-methoxy-6-trifluoromethylchlorobenzene, the reaction was carried out for 3 hours. The reaction mixture was treated as the process of Preparation 6 to obtain 1.4 g. of the object oily compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04331670 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-080000c8c2ec4c20a9611b75fc2e1c26 |
| Source note | uspto-grants-1982_05 |