HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → N-(1-Methyldecyl)-3-(3-Nitrophenyl)-2-butenamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | 2-Undecanamine | HCID 114476 | — |
| Reactant | 3-(3-Nitrophenyl)-2-butenoic acid | HCID 54402156 | — |
| Product | N-(1-Methyldecyl)-3-(3-Nitrophenyl)-2-butenamide | HCID 53905448 | 72% |
Reaction Steps
The 3-(3-nitrophenyl)-2-butenoic acid from Preparation 12 having a melting point of 147°-149° C. was reacted with ethyl chloroformate, followed by 1-methyldecylamine, according to the procedure of Preparation 22. This afforded a 72% yield of the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04331683 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-a8f0524cc10745c4b5996dab7003875b |
| Source note | uspto-grants-1982_05 |