Isopropyl Isothiocyanate → HCID 178456972, compound

HRID 1066120Notes

Reaction equation

HRID 1066120 reaction equation
[NH2:1][C:2]1[C:7]([Cl:8])=[CH:6][C:5]([Cl:9])=[CH:4][C:3]=1[S:10]([NH2:13])(=[O:12])=[O:11].[CH:14]([N:17]=[C:18]=S)([CH3:16])[CH3:15]>>[Cl:8][C:7]1[C:2]2[NH:1][C:18]([NH:17][CH:14]([CH3:16])[CH3:15])=[N:13][S:10](=[O:12])(=[O:11])[C:3]=2[CH:4]=[C:5]([Cl:9])[CH:6]=1

Participants

3

Reactant 2

HCID 75263Isopropyl IsothiocyanateHCID 12248854HCID 12248854, compound

Product 1

HCID 178456972HCID 178456972, compoundYield 17.4%

Procedure

Starting from 2-amino-3,5-dichlorobenzenesulfonamide (0.5 g; 2.07 mmol) and isopropyl isothiocyanate (251 mg; 2.48 mmol) with the use of the procedure described in example 4, 100 mg (17.4%) of the title compound was isolated; m.p. >230° C.

Sources & evidence

ORD record
ord-3296bfb4de624d6fb2910fc750883bea
Source dataset
uspto-grants-2001_06
Patent number
US06242443B1

Reaction notes

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