Isopropyl Isothiocyanate → HCID 178456974, compound

Participants

Reaction Steps

The title compound was prepared from 2-amino-5-chloro-3-nitrobenzenesulfonamide and isopropyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 266-267° C.; 1H-NMR (DMSO-d6): δ 1.20 (d, 6H, CH(CH3)2), 3.92 (m, 1H, CH(CH3)2), 8.19 (d, 1H, ArH), 8.48 (d, 1H, ArH), 8.72 (br.s, 1H, NH), 10.57 (br.s, 1H, NH); MS: m/e 318/320 (M+); (C10H11N4Cl1O4S1) calc. C, 37.68; H, 3.48; N, 17.58, found C, 37.82; H, 3.54; N, 17.58.

Provenance & Evidence