Ethyl Acetate → HCID 178456966, compound

Participants

Reaction Steps

The title compound was prepared from 2-amino-4-trifluoromethylbenzenesulfonamide and isopropyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 294-297° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 1.20 (d, 6H, CH(CH3)2), 3.95 (m, 1H, CH(CH3)2), 7.42 (br., 1H, NH), 7.56 (m, 2H, ArH), 7.99 (d, 1H, ArH), 10.55 (br.s, 1H, NH); MS: m/e 307 (M+, 33%); (C11H12N3F3O2S1.H2O) calc. C, 40.6; H, 4.3; N, 12.9; found C, 41.0; H, 4.1; N, 13.1.

Provenance & Evidence