Isopropyl Isothiocyanate → HCID 178465977, compound

Participants

Reaction Steps

The title compound was prepared from 4-acetyl-2-aminobenzenesulfonamide and isopropyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 305-308° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 1.19 (d, 6H, CH(CH3)2), 3.95 (m, 1H, CH(CH3)2), 7.25 (br., 1H, NH), 7.70-7.85 (m, 3H, ArH), 10.5 (br.s, 1H, NH); MS: m/e 281 (M+; 39%); (C12H15N3O3S1) calc. C, 51.23; H, 5.37; N, 14.94, found C, 51.15; H, 5.50; N, 14.69.

Provenance & Evidence