Isopropylamine → HCID 178456988, compound

HRID 1066143Notes

Reaction equation

HRID 1066143 reaction equation
[NH+]1C=CN[CH:2]=1.[N:6]1([C:11]2[NH:16][C:15]3[CH:17]=[CH:18][C:19]([N+:21]([O-:23])=[O:22])=[CH:20][C:14]=3[S:13](=[O:25])(=[O:24])[N:12]=2)[CH:10]=[CH:9]N=C1.C(N)(C)C>>[CH:10]([NH:6][C:11]1[NH:16][C:15]2[CH:17]=[CH:18][C:19]([N+:21]([O-:23])=[O:22])=[CH:20][C:14]=2[S:13](=[O:25])(=[O:24])[N:12]=1)([CH3:9])[CH3:2]

Participants

3

Reactant 2

HCID 6363IsopropylamineHCID 702374163-(Imidazol-1-yl)-7-nitro-4H-1,2,4-benzothiadiazine 1,1-dioxide imidazolium salt

Product 1

HCID 178456988HCID 178456988, compound

Procedure

3-(Imidazol-1-yl)-7-nitro-4H-1,2,4-benzothiadiazine 1,1-dioxide imidazolium salt was treated with isopropylamine according to the general procedure Method A to give the title compound; m.p. 311-313° C.; IR (KBr): 3363, 3221, 2980, 1657, 1646,1615, 1601, 1572, 1532, 1494, 1339, 1284, 1267, 1155, 1106 cm−1; 1H-NMR (DMSO-d6, HMDS; d ppm): 1.10 (d, 6H, 2×CH3), 3.90 (m, 1H, NH—CH), 7.35 (m, 2H, 5-H+NH—CH), 8.35 (m, 2H, 6-H+8-H), 10.90 (bs, 1H, NH).

Sources & evidence

ORD record
ord-75bf4cbbe9354f7a85b028b0541368c6
Source dataset
uspto-grants-2001_06
Patent number
US06242443B1

Reaction notes

Loading…