Cyclopropanemethanamine → HCID 178526450, compound

HRID 1066146Notes

Reaction equation

HRID 1066146 reaction equation
[NH+]1[CH:5]=[CH:4]NC=1.[N:6]1([C:11]2[NH:16][C:15]3[CH:17]=[CH:18][C:19]([N+:21]([O-:23])=[O:22])=[CH:20][C:14]=3[S:13](=[O:25])(=[O:24])[N:12]=2)[CH:10]=[CH:9]N=C1.C1(CN)CC1>>[CH:9]1([CH2:10][NH:6][C:11]2[NH:16][C:15]3[CH:17]=[CH:18][C:19]([N+:21]([O-:23])=[O:22])=[CH:20][C:14]=3[S:13](=[O:24])(=[O:25])[N:12]=2)[CH2:5][CH2:4]1

Participants

3

Reactant 2

HCID 75646CyclopropanemethanamineHCID 702374163-(Imidazol-1-yl)-7-nitro-4H-1,2,4-benzothiadiazine 1,1-dioxide imidazolium salt

Product 1

HCID 178526450HCID 178526450, compound

Procedure

3-(Imidazol-1-yl)-7-nitro-4H-1,2,4-benzothiadiazine 1,1-dioxide imidazolium salt was treated with cyclopropylmethylamine according to the general procedure Method D to give the title compound; m.p.: 276-278° C.; IR (KBr): 3290, 3193, 3104, 2994, 1635, 1603,1564, 1539, 1499, 1486, 1347, 1276, 1251,1153, 1111 cm−1.

Sources & evidence

ORD record
ord-99f3600c7c5b4e098ac71498895f88b7
Source dataset
uspto-grants-2001_06
Patent number
US06242443B1

Reaction notes

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