HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 1-Adamantaneacetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1-Adamantaneacetic acid | HCID 123221 | — |
| Product | 1-Adamantaneacetyl chloride | HCID 2771882 | — |
Reaction Steps
A solution of 1-adamantaneacetic acid (4.5 g) in thionyl chloride (20 ml) was heated at reflux temperature for 24 hours and then allowed to cool to ambient temperature. The excess thionyl chloride was removed under reduced pressure to leave the sub-title compound as a syrup (4.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06242470B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-b40ced9f6fb044bb8469205389c0df57 |
| Source note | uspto-grants-2001_06 |