2,4,5-Trimethylaniline → HCID 9861553, compound

HRID 1066234Notes

Reaction equation

HRID 1066234 reaction equation
[C:1]12([CH2:11][C:12](Cl)=[O:13])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[CH3:15][C:16]1[CH:22]=[C:21]([CH3:23])[C:20]([CH3:24])=[CH:19][C:17]=1[NH2:18]>>[CH3:15][C:16]1[CH:22]=[C:21]([CH3:23])[C:20]([CH3:24])=[CH:19][C:17]=1[NH:18][C:12](=[O:13])[CH2:11][C:1]12[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2

Participants

3

Reactant 2

HCID 87172,4,5-TrimethylanilineHCID 27718821-Adamantaneacetyl chloride

Product 1

HCID 9861553HCID 9861553, compoundYield 14.3%

Procedure

Prepared according to the method of Example 1b) from 1-adamantaneacetyl chloride (0.2 g) and 2,4,5-trimethylaniline (0.13 g) to give the title compound as a white solid (0.042 g).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-31ab53628d184405b1d4b5f31c6603fd
Source dataset
uspto-grants-2001_06
Patent number
US06242470B1

Reaction notes

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