3,5-Dimethoxyaniline → HCID 4539226, compound

HRID 1066262Notes

Reaction equation

HRID 1066262 reaction equation
[C:1]12([CH2:11][C:12](O)=[O:13])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[CH3:15][O:16][C:17]1[CH:18]=[C:19]([CH:21]=[C:22]([O:24][CH3:25])[CH:23]=1)[NH2:20]>>[CH3:25][O:24][C:22]1[CH:21]=[C:19]([NH:20][C:12](=[O:13])[CH2:11][C:1]23[CH2:8][CH:7]4[CH2:9][CH:3]([CH2:4][CH:5]([CH2:6]4)[CH2:10]2)[CH2:2]3)[CH:18]=[C:17]([O:16][CH3:15])[CH:23]=1

Participants

3

Reactant 2

HCID 663013,5-DimethoxyanilineHCID 1232211-Adamantaneacetic acid

Product 1

HCID 4539226HCID 4539226, compoundYield 82.6%

Procedure

Prepared according to the method of Example 39 from 1-adamantaneacetic acid (3.0 g) and 3,5-dimethoxyaniline (3.0 g) to give the title compound as a white solid (4.2 g).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-6c556e87c7be43338e67019cf95911cf
Source dataset
uspto-grants-2001_06
Patent number
US06242470B1

Reaction notes

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