HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → (1-Acetylpiperidin-4-yl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 4-Piperidineacetic acid | HCID 1512594 | — |
| Product | (1-Acetylpiperidin-4-yl)acetic acid | HCID 10442408 | 99% |
Reaction Steps
4-Piperidinylacetic acid (5 grams) (35.0 mmoles) was reacted with acetic anhydride (10.7 grams) (105.0 mmoles) as described in Preparative Example 13A to give the title compound (Yield: 6.4 grams, 99%, MH+ 185).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06242458B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-ecff1cd7cec64851b616981603e56170 |
| Source note | uspto-grants-2001_06 |