HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178520291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | bromine AcOH | HCID 87433071 | — |
| Reactant | HCID 178520292 | HCID 178520292 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178520291 | HCID 178520291 | 71% |
Reaction Steps
To a solution of the title compound from Example 252 (0.19 grams) and glacial acetic acid (4 mL) was added a 0.7 M bromine-acetic acid solution (0.7 mL) at 25° C. under N2. After 10 minutes, water was added and the resulting solid was filtered and washed with water several times and dried to give the title compound (0.18 grams, 71%, MH+ 526).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06242458B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-bb1ed66608cf4fccae0ed912d0e36e34 |
| Source note | uspto-grants-2001_06 |