Trifluoroacetic acid → HCID 88213892, compound

Participants

Reaction Steps

A solution of N,N′-bis[6-chloro-2-(tert-butoxycarbonyl)methoxy-9-acridinyl]-1,2-ethanediamine (12 mg, 0.12 mmol) and trifluoroacetic acid (5 mL) in dichloromethane (12 mL) was stirred at RT for 18 h. The reaction mixture was concentrated in vacuo and the residue was purified by HPLC (YMC ODS-AQ, 100×250 mm, 80 mL/min, 26% acetonitrile/water/0.1% trifluoroacetic acid, UV detection at 254 nm) to give the title compound as a yellow solid. MS(ES) m/e 631.3 (M+H)+.

Provenance & Evidence