Palmitoyl chloride → HCID 21199999, compound

HRID 1066376Notes

Reaction equation

HRID 1066376 reaction equation
[NH2:1][C:2]1[C:6]([NH2:7])=[CH:5][S:4][CH:3]=1.[C:8](Cl)(=[O:24])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23]>C1(C)C=CC=CC=1.CCCCCC>[C:8]([NH:1][C:2]1[C:6]([NH:7][C:8](=[O:24])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])=[CH:5][S:4][CH:3]=1)(=[O:24])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23]

Participants

4

Reactant 2

HCID 8206Palmitoyl chlorideHCID 643216Thiophene-3,4-diamine

Product 1

HCID 21199999HCID 21199999, compoundYield 70%

Reagents, catalysts & solvents 1

HCID 21889329Toluene hexaneSolvent

Procedure

This compound was prepared in a yield of 70% of theory starting from 3,4-diaminothiophene and palmitoyl chloride (boiling point 141° C. at 1.4 mbar) in a similar manner to above. The melting point was 107-109° C. (from toluene-hexane).

Workup

  1. customThis compound was prepared in a yield of 70% of theory

Sources & evidence

ORD record
ord-4b389981099f4a848b511269e064182e
Source dataset
uspto-grants-2001_06
Patent number
US06242561B1

Reaction notes

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