HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Methyl 2-benzylidene-3-hydroxypropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 2-[(acetyloxy)methyl]-3-phenylprop-2-enoate | HCID 53678280 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 2-benzylidene-3-hydroxypropionate | HCID 54265908 | — |
Reaction Steps
The crude product (2.1917 g) of methyl 2-benzylidene-3-acetoxypropionate obtained in Example 13 was dissolved in 15 ml of methanol, and 84 mg (97%, 2.04 mmols) of sodium hydroxide were added thereto. The mixture was stirred at room temperature for 4 hours to form methyl 2-benzylidene-3-hydroxypropionate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06242635B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-c62619cd183b43d4b504d2fff2143bda |
| Source note | uspto-grants-2001_06 |