HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → HCID 21195365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | 2-propyl-1,3-dithiane | HCID 11062707 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 21195365 | HCID 21195365 | 86.9% |
Reaction Steps
The synthesis was carried out in a similar manner to Example 4/(a), but using 8 g (49.3 mmol) of 2-n-propyl-1,3-dithian, 52 mmol of n-butyllithium (32.5 ml of a 1.6 M solution in n-hexane) and 2.5 g (56.8 mmol) of acetaldehyde. 8.84 g of 2-(1-hydroxyethyl)-2-n-propyl-1,3-dithian were obtained as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245328B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-b923f836d96c47f28735adfde80c44ff |
| Source note | uspto-grants-2001_06 |