HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 18551156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 17935607 | HCID 17935607 | — |
| Catalyst | Zinc cyanide (Zn(CN)2) | HCID 11186 | — |
| Product | HCID 18551156 | HCID 18551156 | — |
Reaction Steps
From 4-(4-bromophenyl)-2-hydroxy-4-methyl-2-trifluoromethyl-valeric acid ethyl ester, zinc cyanide and tetrakis-triphenylphosphine-palladium in dimethylformamide at 140° C. After saponification, the title acid is obtained as a foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245804B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-291ded54d9854e849005133dc9efca32 |
| Source note | uspto-grants-2001_06 |