HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 18551182, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 17935632 | HCID 17935632 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18551182 | HCID 18551182 | — |
Reaction Steps
From 2-hydroxy-4-(4-methoxyphenyl)-4-methyl-2-trifluoromethyl-valeric acid ethyl ester by bromation with N-bromosuccinimide in dimethylformamide at 0° C. and subsequent saponification. Melting point 94-96° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245804B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-f6943c052605416ea0abc3a5456414da |
| Source note | uspto-grants-2001_06 |