HRID1067030

反应详情

EQUATION

反应方程式

HRID 1067030 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
27.5 °C

PROCEDURE

实验过程

To a suspension of urea (80 g, 1.333 mols) in acetic acid (100 ml), iminostilbene hydrochloride (20.5 g, 0.089 mols) was added under stirring at 25-30° C. The resulting reaction mixture was worked up according to the method of Example 1 to produce carbamazepine, which was identical to the product of Example 1.

WORKUP

后处理

  1. additionwas added
  2. customThe resulting reaction mixture