HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylimidazole → 1-Butyl-3-ethylimidazolium hexafluorophosphat
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylimidazole | HCID 61347 | — |
| Reactant | Oxonium, triethyl-, hexafluorophosphate(1-) (1:1) | HCID 167684 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | 1-Butyl-3-ethylimidazolium hexafluorophosphat | HCID 21196968 | — |
Reaction Steps
1.1 ml of N-butylimidazole was introduced into a 50 ml glass flask under an argon atmosphere. 2.08 g of triethyloxonium hexafluorophosphate in solution in 5 ml of 1,2-dichloroethane was then introduced. The mixture was stirred for 4 hours at room temperature. The solvent was evaporated off under vacuum using a vane pump. A colorless liquid was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245918B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-f99328f2848a4266b5576827d686e797 |
| Source note | uspto-grants-2001_06 |