HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 131722649, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 122173709 | HCID 122173709 | — |
| Product | HCID 131722649 | HCID 131722649 | — |
Reaction Steps
This compound is prepared using Procedure C. Nα-Boc-Nδ-Fmoc-Nα-methylornithine (100 mg) was coupled with benzylamine to afford titled compound (50 mg) as a glassy solid: 1H NMR (400 MHz, CDCl3) δ1.42 (s, 9H), 1.52 (m, 2H), 1.70 (m, 2H), 2.80 (s, 3H), 3.26 (m, 2H), 4.18 (m, 1H), 4.22 (m, 1H), 4.41 (m, 2H), 4.61 (m, 2H), 7.31 (m, 7H), 7.43 (m, 2H), 7.63 (m, 2H), and 7.81 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245746B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-470e08592c2d4454ad79993d45f7f4e6 |
| Source note | uspto-grants-2001_06 |