Ethyl acetimidate → HCID 178465613, compound

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Reaction Steps

Glycyl-Nα-(phenethyl)ornithine 3-phenylpropylamide trifluoroacetate was treated with ethyl acetimidate in ethanol at pH9 and the product was purified by HPLC: 1H NMR (400 MHz, D2O) δ1.6-2.0 (m, 6H), 2.3 (s, 3H), 2.7 (t, J=6.4 Hz, 2H), 2.9-3.1 (m, 4H), 3.2-3.4 (m, 2H), 3.5-3.7 (m, 2H), 4.1-4.3 (m, 2H), 4.7-4.8 (m, 1H), and 7.2-7.5 (m, 10H); mass spectrum, m/e 453 (M+), 354, 300, 247, and 219.

Provenance & Evidence