Acrylonitrile → HCID 14791345, compound

HRID 1067088Notes

Reaction equation

HRID 1067088 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][NH2:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:11](#[N:14])[CH:12]=[CH2:13]>C(O)C>[C:11]([CH2:12][CH2:13][NH:10][CH2:9][CH2:8][CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)#[N:14]

Participants

4

Reactant 2

HCID 7855AcrylonitrileHCID 162593-Phenylpropylamine

Product 1

HCID 14791345HCID 14791345, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of 3-phenylpropylamine (0.95 g, 7 mmol) and acrylonitrile (0.55 ml, 8.4 mmol) in ethanol (30 ml) was refluxed for 2 hours to give N-(2-cyanoethyl)-3-phenyl-propylamine.

Workup

  1. temperaturewas refluxed for 2 hours

Sources & evidence

ORD record
ord-e778e8bd4449421a97b141a5c8e17628
Source dataset
uspto-grants-2001_06
Patent number
US06245746B1

Reaction notes

Loading…