HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9888387, compound → HCID 21196512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9888387 | HCID 9888387 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21196512 | HCID 21196512 | 71.7% |
Reaction Steps
3-{[2-(4,5-Diphenyloxazol-2-yl)-2-cyclopenten-1-yl]-methyl}benzamide (75 mg) was hydrogenated over 5% Pd/C (3 mg) in methanol (20 ml) at room temperature at 3 atm for 7 hours. The mixture was filtered and the filtrate was evaporated in vacuo. The residue was triturated with a mixture of ether and n-hexane to afford 3-{[2-(4,5-diphenyloxazol-2-yl)-1-cyclopentyl]methyl}benzamide (54 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245790B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-0d7bfb1053624cd4879a43e7c37f26e0 |
| Source note | uspto-grants-2001_06 |