HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → HCID 57708186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 5-Nitrosalicylic acid | HCID 7318 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 57708186 | HCID 57708186 | — |
Reaction Steps
40 g (218.4 mmol) of 2-hydroxy-5-nitro-benzoic acid, 236.17 g (2.184 mol) of benzyl alcohol and 1 g of p-toluenesulfonic acid in 1000 ml of toluene are heated for 2 days in a water separator. It is evaporated to dryness and the residue is chromatographed on silica gel (mobile solvent: methylene chloride/hexane/acetone=15:5:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248306B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-4881ec995f154d0d9007ea4904e4a96e |
| Source note | uspto-grants-2001_06 |