HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 4-Methoxy-3-(trifluoromethyl)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-Methoxy-3-(trifluoromethyl)benzoic acid | HCID 2775295 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 4-Methoxy-3-(trifluoromethyl)benzoyl chloride | HCID 2775298 | — |
Reaction Steps
The title compound was prepared from 4-methoxy-3-trifluoromethylbenzoic acid with oxalyl chloride and DMF in chloroform at room temperature [D. Levin, Chem. Br., 1977, 20] followed by evaporation in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248754B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-c8bed219f5004b4ab64c9b40200868a5 |
| Source note | uspto-grants-2001_06 |