HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Biphenyl, 4-(bromomethyl)- → [[2-(4-Phenylbenzylthio)-4,5-dihydronaphtho[1,2-d]thiazol-6-yl]oxy]acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Biphenyl, 4-(bromomethyl)- | HCID 257716 | — |
| Reactant | Ethyl[(2-mercapto-4,5-dihydronaphtho[1,2-d]thiazol-6-yl)oxy)acetate | HCID 178472952 | — |
| Product | [[2-(4-Phenylbenzylthio)-4,5-dihydronaphtho[1,2-d]thiazol-6-yl]oxy]acetic acid | HCID 70116980 | 68% |
Reaction Steps
Using ethyl[(2-mercapto-4,5-dihydronaphtho[1,2-d]thiazol-6-yl)oxy)acetate and 4-phenylbenzyl bromide, the procedure of Example 1 was otherwise repeated to synthesize the title compound. Yield 68%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248766B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-4b09df28b932460fb5ac7f097a337c56 |
| Source note | uspto-grants-2001_06 |