3,3-Diphenylpropyl iodide → HCID 54115040, compound
Reaction equation
C([O:3][C:4](=[O:22])[CH2:5][O:6][C:7]1[C:8]2[CH2:9][C:10]3[S:14][C:13]([SH:15])=[N:12][C:11]=3[C:16]=2[C:17]([CH3:21])=[C:18]([CH3:20])[CH:19]=1)C.[C:23]1([CH:29]([C:33]2[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=2)[CH2:30][CH2:31]I)[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>>[C:23]1([CH:29]([C:33]2[CH:34]=[CH:35][CH:36]=[CH:37][CH:38]=2)[CH2:30][CH2:31][S:15][C:13]2[S:14][C:10]3[CH2:9][C:8]4[C:7]([O:6][CH2:5][C:4]([OH:3])=[O:22])=[CH:19][C:18]([CH3:20])=[C:17]([CH3:21])[C:16]=4[C:11]=3[N:12]=2)[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1Participants
3
Procedure
Using ethyl[(2-mercapto-4,5-dimethyl-8H-indeno[1,2-d]thiazol-7-yl)oxy]acetate and 3,3-diphenylpropyl iodide, the procedure of Example 21 was otherwise repeated to synthesize the title compound. Yield 53%.
Sources & evidence
- ORD record
- ord-0fc25e463d8545378e29786333c7eb7a
- Source dataset
- uspto-grants-2001_06
- Patent number
- US06248766B1
Reaction notes
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