HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 21193924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21193840 | HCID 21193840 | — |
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 21193924 | HCID 21193924 | 99% |
Reaction Steps
Yield: 99% of theory, Rf value: 0.21 (silica gel; methylene chloride/methanol=4:1+1% glacial acetic acid); C26H33N7O3×HCl (491.60/528.05). mass spectrum: ( M + H ) + = 492 ( M - H + HCl ) - = 526 / 8 ( Cl ) ( M - H + 2 HCl ) - = 562 / 4 / 8 ( Cl 2 )
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248770B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-d1bb3dd592dd412f996396796e459f11 |
| Source note | uspto-grants-2001_06 |