2-Methylbenzimidazole → HCID 21193815, compound

HRID 1067473Notes

Reaction equation

HRID 1067473 reaction equation
[CH3:1][C:2]1[NH:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[Cl:11][C:12]1[CH:19]=[CH:18][C:15]([CH2:16]Cl)=[CH:14][C:13]=1[N+:20]([O-:22])=[O:21]>CS(C)=O>[Cl:11][C:12]1[CH:19]=[CH:18][C:15]([CH2:16][N:3]2[C:4]3[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=3[N:6]=[C:2]2[CH3:1])=[CH:14][C:13]=1[N+:20]([O-:22])=[O:21]

Participants

4

Reactant 2

HCID 119842-MethylbenzimidazoleHCID 936621-Chloro-4-(chloromethyl)-2-nitrobenzene

Product 1

HCID 21193815HCID 21193815, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent

Procedure

Prepared analogously to Example 9a from 2-methyl-benzimidazole and 4-chloro-3-nitrobenzyl chloride in dimethylsulphoxide.

Sources & evidence

ORD record
ord-18ae541ef20342689e3f502e1a550b84
Source dataset
uspto-grants-2001_06
Patent number
US06248770B1

Reaction notes

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