HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-1-propanol → HCID 11769376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-1-propanol | HCID 9086 | — |
| Reactant | 6-Chloro-(1,2,4)triazolo(1,5-b)pyridazine | HCID 11240611 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 11769376 | HCID 11769376 | 72% |
Reaction Steps
6-Chloro[1,2,4]triazolo[1,5-b]pyridazine (928 mg) was dissolved in ethanol (10 ml). 3-Amino-1-propanol (1.23 g) was added to the solution. The mixture was refluxed under heating for 20 hours. After being cooled, the mixture was concentrated under reduced pressure to an half of its volume. The resulting precipitates were washed with ethanol and dried to yield the title compound (835 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248740B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-6b5b66a1f771403291715d52df72b1b7 |
| Source note | uspto-grants-2001_06 |