Allyl bromide → HCID 178459060, compound
Reaction equation
C1(C(C2C=CC=CC=2)(C2C=CC=CC=2)[N:8]2[CH:12]=[C:11]([CH2:13][CH2:14][CH2:15][OH:16])[N:10]=[CH:9]2)C=CC=CC=1.Br[CH2:30][CH:31]=[CH2:32]>>[CH2:32]([O:16][CH2:15][CH2:14][CH2:13][C:11]1[N:10]=[CH:9][NH:8][CH:12]=1)[CH:31]=[CH2:30]Participants
3
Procedure
5 mmol of 3-(1-triphenylmethyl-1H-imidazol-4-yl)propanol and 5 mmol of 3-bromo-1-propene are treated as described in Example 5. The title compound is crystallized in the form of the hydrogen oxalate from ethanol and diethyl ether.
Workup
- customThe title compound is crystallized in the form of the hydrogen oxalate from ethanol and diethyl ether
Sources & evidence
- ORD record
- ord-bf3bd79ab4e840259c11ad8f63f5cd7e
- Source dataset
- uspto-grants-2001_06
- Patent number
- US06248765B1
Reaction notes
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