Propargyl bromide → HCID 178459059, compound

HRID 1067703Notes

Reaction equation

HRID 1067703 reaction equation
C1(C(C2C=CC=CC=2)(C2C=CC=CC=2)[N:8]2[CH:12]=[C:11]([CH2:13][CH2:14][CH2:15][OH:16])[N:10]=[CH:9]2)C=CC=CC=1.Br[CH2:30][C:31]#[CH:32]>>[CH2:32]([O:16][CH2:15][CH2:14][CH2:13][C:11]1[N:10]=[CH:9][NH:8][CH:12]=1)[C:31]#[CH:30]

Participants

3

Reactant 2

HCID 7842Propargyl bromideHCID 108328403-(1-Trityl-1H-imidazol-4-YL)propan-1-OL

Product 1

HCID 178459059HCID 178459059, compound

Procedure

5 mmol of 3-(1-triphenylmethyl-1H-imidazol-4-yl)propanol and 5 mmol of 3-bromo-1-propyne are treated as described in Example 5. The title compound is crystallized in the form of the hydrogen oxalate from ethanol and diethyl ether.

Workup

  1. customThe title compound is crystallized in the form of the hydrogen oxalate from ethanol and diethyl ether

Sources & evidence

ORD record
ord-62c18523eb4b49af93eb222029835abe
Source dataset
uspto-grants-2001_06
Patent number
US06248765B1

Reaction notes

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