4-(1-Pentynyl)phenol → HCID 178442188, compound
Reaction equation
C(OC([N:8]1[CH:12]=[C:11]([CH2:13][CH2:14][CH2:15][OH:16])[N:10]=[CH:9]1)=O)(C)(C)C.[C:17]([C:22]1[CH:27]=[CH:26][C:25](O)=[CH:24][CH:23]=1)#[C:18][CH2:19][CH2:20][CH3:21]>>[C:17]([C:22]1[CH:23]=[CH:24][C:25]([O:16][CH2:15][CH2:14][CH2:13][C:11]2[N:10]=[CH:9][NH:8][CH:12]=2)=[CH:26][CH:27]=1)#[C:18][CH2:19][CH2:20][CH3:21]Participants
3
Procedure
5 mmol of 4-(3-hydroxypropyl)-1H-imidazole-1-carboxylic acid tert-butyl ester and 5 mmol of 4-(1-pentynyl)phenol are treated as described in Example 122.
Sources & evidence
- ORD record
- ord-798f203aed81402198dbdf403867ae24
- Source dataset
- uspto-grants-2001_06
- Patent number
- US06248765B1
Reaction notes
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