HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 3,4-Dimethyl-2-nitrophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 3,4-Dimethylphenol | HCID 7249 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3,4-Dimethyl-2-nitrophenol | HCID 13571454 | — |
Reaction Steps
The reaction was carried out in a manner similar to Reference Example 20 a) except for using 15.7 g (129 mmol) of 3,4-dimethylphenol, 130 ml of acetic acid, 8 ml of water and 12.2 g (135 mmol) of 70% nitric acid. 3,4-Dimethyl-2-nitrophenol was thus obtained in the yield of 7.01 g (26.0%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248772B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-95563cda57a146e1a931ce3e7d3335f1 |
| Source note | uspto-grants-2001_06 |