HRID1068088

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID3092607

未命名化合物

HCID178418668

未命名化合物

PRODUCTS

生成物

结构：COc1cc(C=NNC(=N)N)ccc1OCCOc1ccc(C=NNC(=N)N)cc1OC.Cl.Cl

HCID178492417

未命名化合物

收率 98.4%

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID178478830

未命名化合物

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

4,4′-(ethylenedioxy)di-m-anisaldehyde (0.99 g), aminoguanidine hydrochloride (0.829 g), and aminoguanidine dihydrochloride (0.01 g) were heated in 95% methanol (10.5 mL) under nitrogen for 16 hr. Cooling and filtration gave 1.52 g of 4,4′-(ethylenedioxy)di-m-anisaldehyde bis(amidinohydrazone) dihydrochloride, mp 322-3° C. dec.

WORKUP

后处理

temperatureCooling
filtrationfiltration