HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → 1-(4-((2,4-Difluorophenyl)-hydroxyimino-methyl)piperidin-1-yl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 1-Acetyl-4-(2',4'-difluorobenzoyl)piperidine | HCID 2740707 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(4-((2,4-Difluorophenyl)-hydroxyimino-methyl)piperidin-1-yl)ethanone | HCID 86757024 | — |
Reaction Steps
The title compound was prepared from 1-(4-(2,4-difluoro-benzoyl)piperidin-1-yl)ethanone, hydroxylamine hydrochloride and sodium acetate in refluxing EtOH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248755B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-9d76206c853e40cb8a895999c76ca2a1 |
| Source note | uspto-grants-2001_06 |