HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → N,N-Diethyl-2,5-difluorobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 2,5-Difluorobenzoyl chloride | HCID 588082 | — |
| Product | N,N-Diethyl-2,5-difluorobenzamide | HCID 5044848 | 94% |
Reaction Steps
Diethyl amine (15.4 g, 210 mmol) and 2,5-difluorobenzoyl chloride (17.6 g, 100 mmol) were reacted using General Method E1 to afford 20.0 g of N,N-diethyl-2,5-difluorobenzamide as a clear oil, a 94% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248894B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-59cae73e1b5546b2aff5f05c67ae0eb3 |
| Source note | uspto-grants-2001_06 |